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固溶冷卻速度和前處理對新型鎳基粉末高溫合金組織與顯微硬度的影響
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國家武器裝備預(yù)研基金 (9140A12070507QT0202);國家高技術(shù)研究發(fā)展計劃 (2007AA03A223)


Effect of Solution Cooling Rate and Pre-heat Treatment on the Microstructure and Microhardness of a Novel Type Nickel-Based P/M Superalloy
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    摘要:

    對新型鎳基粉末高溫合金FGH98Ⅰ分別進行亞固溶前處理+過固溶和過固溶熱處理,利用光學(xué)顯微鏡,場發(fā)射掃描電鏡和顯微硬度儀研究冷卻速度對合金組織與顯微硬度的影響。結(jié)果表明:過固溶處理前的亞固溶前處理使鍛態(tài)合金中大晶界γ′相發(fā)生部分溶解,晶粒稍有長大,對過固溶熱處理冷卻γ′相析出的影響不顯著;隨著冷速增加,合金中二次和三次γ′相的尺寸減小,二次γ′相的形狀從蝶形向球形轉(zhuǎn)變,γ′相的顆粒密度增大,面積分數(shù)減小,在冷卻速度≤1.4 ℃/s時,γ′相分兩階段形核;冷速越快,合金的硬度越高,時效后硬度增高越多。另外,還建立了冷速與γ′相平均尺寸和合金硬度之間的函數(shù)關(guān)系式。該結(jié)果為FGH98Ⅰ合金實際雙性能盤固溶熱處理工藝的選擇提供了理論參考

    Abstract:

    The effect of solution cooling rate on the microstructure and microhardness of a novel type nickel-based P/M superalloy FGH98Ⅰin subslovus plus superslovus and superslovus heat treatment condition was studied by means of optical microscope (OM), field emission scanning electron microscope (FESEM) and microhardness tester. The results show that subslovus pre-heat treatment makes the large grain boundary γ ' phase of as-forged alloy partial dissolution, and the grains grow a little, while the influence on the cooling γ ' precipitates of superslovus heat treatment is not obvious. The average sizes of secondary and tertiary γ ' precipitates decrease with the cooling rate increasing. Meanwhile, the shape of secondary γ ' precipitates changes from the butterfly-like to the spherical, the γ ' phase particle density increases and the area fraction decreases. It is also found that γ ' phases nucleate and precipitate in two stages if the cooling rate is not faster than 1.4 °C/s. The higher the cooling rate, the higher the microhardness, and the microhardness increases more after aging. In addition, the average sizes of γ′ precipitates and the microhardness as a function of cooling rate are established. The above results can be used as a theoretical reference for the selection of actual superslovus processing of FGH98Ⅰdual-property disk

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吳 凱,劉國權(quán),胡本芙,張義文,陶 宇,劉建濤.固溶冷卻速度和前處理對新型鎳基粉末高溫合金組織與顯微硬度的影響[J].稀有金屬材料與工程,2012,41(4):685~691.[Wu Kai, Liu Guoquan, Hu Benfu, Zhang Yiwen, Tao Yu, Liu Jiantao. Effect of Solution Cooling Rate and Pre-heat Treatment on the Microstructure and Microhardness of a Novel Type Nickel-Based P/M Superalloy[J]. Rare Metal Materials and Engineering,2012,41(4):685~691.]
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  • 收稿日期:2011-04-09
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