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120°模具室溫ECAP制備工業(yè)純鈦的熱壓縮變形行為
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國(guó)家自然科學(xué)基金 (50874086); 高等學(xué)校博士學(xué)科點(diǎn)專項(xiàng)科研基金 (20116020110012); 陜西省自然科學(xué)基金 (2010JM6010)


Hot Compression Deformation Behavior of as-ECAPed CP-Ti at Room Temperature with 120° Die
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    摘要:

    在Gleeble-1500熱模擬機(jī)上對(duì)室溫120°模具等徑彎曲通道變形(ECAP)制備的平均晶粒尺寸為200 nm的工業(yè)純鈦(CP-Ti)進(jìn)行等溫變速壓縮實(shí)驗(yàn),研究超細(xì)晶(UFG)工業(yè)純鈦在變形溫度為298~673 K和應(yīng)變速率為10-3~100 s-1條件下的流變行為。利用透射電子顯微鏡分析超細(xì)晶工業(yè)純鈦在不同變形條件下的組織演化規(guī)律。結(jié)果表明:流變應(yīng)力在變形初期隨應(yīng)變的增加而增大,出現(xiàn)峰值后逐漸趨于平穩(wěn);峰值應(yīng)力隨溫度的升高而減小,隨應(yīng)變速率的增大而增大;隨變形溫度的升高和應(yīng)變速率的降低,應(yīng)變速率敏感性指數(shù)m增加,晶粒粗化,亞晶尺寸增大,再結(jié)晶晶粒數(shù)量逐漸增加;超細(xì)晶工業(yè)純鈦熱壓縮變形的主要軟化機(jī)制隨變形溫度的升高和應(yīng)變速率的降低由動(dòng)態(tài)回復(fù)逐步轉(zhuǎn)變?yōu)閯?dòng)態(tài)再結(jié)晶

    Abstract:

    Hot compression deformation behavior of Ultrafine-grained (UFG) commercially pure (CP) Ti with the average grain size of 200 nm was studied by thermal simulation test at the deformation temperature of 298-673 K and the strain rate of 10-3-100 s-1 on the Gleeble-1500 thermal-mechanical simulator. UFG CP-Ti was produced by ECAP up to 8 passes with a die of Φ=120° using route Bc at room temperature. The microstructural evolution of UFG CP-Ti was investigated by transmission electron microscopy. The results show that the flow stress increases with increasing of strain and tends to be constant after a peak value. The peak stress increases with increasing of strain rate and decreases with increasing of deformation temperature. Strain rate sensitivity value m of the UFG CP-Ti is found to increase with increasing of temperature and decreasing of strain rate. And the grains in the deformed samples are coarsened and the size of subgrains increases; the number of fine grains in grain boundaries also increases, indicating that the main softening mechanism of the alloy during hot compression deformation is attributed to the transformation from dynamic recovery to dynamic recrystallization

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劉曉燕,趙西成,楊西榮,王 成.120°模具室溫ECAP制備工業(yè)純鈦的熱壓縮變形行為[J].稀有金屬材料與工程,2012,41(4):667~671.[Liu Xiaoyan, Zhao Xicheng, Yang Xirong, Wang Cheng. Hot Compression Deformation Behavior of as-ECAPed CP-Ti at Room Temperature with 120° Die[J]. Rare Metal Materials and Engineering,2012,41(4):667~671.]
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  • 收稿日期:2011-04-08
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