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冷加工態(tài)Ti6Al4V合金的回復和再結(jié)晶行為研究
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中央高?;究蒲袠I(yè)務費專項資金(DUT10ZDG02)


Recovery and Recrystallization Behavior of Ti6Al4V Alloys after Cold Deformation
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    摘要:

    對冷拉拔變形量為60%的鈦合金進行700~880 ℃,1~240 min再結(jié)晶退火,利用金相顯微鏡、X射線衍射儀和透射電鏡等手段分析不同狀態(tài)下的組織演變、織構(gòu)組成和位錯組態(tài)。結(jié)果表明:冷變形后的Ti6Al4V合金經(jīng)完全再結(jié)晶后α晶粒呈等軸狀,β相在α相周圍以條狀沿α晶界析出或以小晶粒形式存在。計算表明,經(jīng)60%冷變形量的鈦合金再結(jié)晶激活能為107 kJ/mol,較相同變形量的純鈦再結(jié)晶激活能高約50%。鈦合金的再結(jié)晶分為回復、形核和晶核長大階段,包括位錯胞向亞晶轉(zhuǎn)變、回復亞晶通過合并或長大形核、形核誘導高角度晶界形成而長大成新晶粒。經(jīng)過冷拉拔后的絲材,存在著較強的 <10

    Abstract:

    The microstructure evolution, crystallographic texture and dislocation configuration during recrystallization of the cold-drawn Ti6Al4V alloy were investigated by optical microscope (OM), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Recrystallization treatment in the 60% cold worked samples was carried out at various temperatures between 700 oC and 880 oC and holding time from 1 min to 240 min. The results demonstrate that recrystallization of the 60% cold-drawn alloy and subsequent grain growth have led α phase to fine equiaxed grains, while β phase distribute along grain boundaries of the α-phase in strip shape or small grains. The value of recrystallization activation energy of the alloy after 60% cold deformation is 107 kJ/mol, which is about 50% higher than that of the deformed pure titanium experienced the equal deformation. The microstructure evolution at different grain stages can be classified as recoveration, nucleation and grain growth stages. It is shown that the recovery involves rearrangement of dislocation cells into subgrains, formation of nuclei through growth or coalescence of subgrains, and growth of nuclei by high angle boundary migration during the annealing of the Ti6Al4V alloy. The as-cold drawn wires present strong <10

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薛 超,胡建軍,陳國清,周文龍,張久文.冷加工態(tài)Ti6Al4V合金的回復和再結(jié)晶行為研究[J].稀有金屬材料與工程,2012,41(3):472~476.[Xue Chao, Hu Jianjun, Chen Guoqing, Zhou Wenlong, Zhang Jiuwen. Recovery and Recrystallization Behavior of Ti6Al4V Alloys after Cold Deformation[J]. Rare Metal Materials and Engineering,2012,41(3):472~476.]
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  • 收稿日期:2011-03-20
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