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固溶溫度對FGH95鎳基合金持久斷裂機制的影響
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國家自然科學(xué)基金(50571070);遼寧省教育廳基金(2004C004)


Effects of Solution Temperatures on Enduring Fracture Mechanism of FGH95 Nickel-Base Superalloy
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    摘要:

    通過對不同溫度固溶處理的FGH95合金進行組織形貌觀察及持久性能測試,研究了組織結(jié)構(gòu)對合金持久性能及其斷裂機制的影響。結(jié)果表明:經(jīng)1150 ℃固溶和時效處理后,合金中有粗大g ¢相在較寬的邊界區(qū)域不連續(xù)分布,其周圍存在g ¢相貧化區(qū);經(jīng)1160 ℃固溶及時效處理后,合金中粗大g ¢相完全溶解,在晶內(nèi)彌散分布高體積分數(shù)的g ¢相,并有粒狀 (Nb, Ti)C碳化物在晶內(nèi)及沿晶界不連續(xù)析出;經(jīng)1165 ℃固溶和時效后,合金的晶粒尺寸明顯長大,并有硬而脆的碳化物膜沿晶界連續(xù)析出。在650 ℃/1034 MPa條件下,經(jīng)1160 ℃固溶和時效的合金,由于在晶界處不連續(xù)析出的粒狀碳化物對晶界具有釘扎作用,可有效阻礙晶界滑移,使合金具有較好的抗蠕變性能。合金蠕變后期的變形特征是晶內(nèi)發(fā)生單取向和雙取向滑移,隨著蠕變進行,滑移跡線增多,并在晶界處引起應(yīng)力集中,致使裂紋在晶界處萌生及擴展并最終導(dǎo)致斷裂。

    Abstract:

    By means of the enduring properties measurement and microstructure observation, the influence of the microstructure on the enduring properties and fracture mechanism for FGH95 nickel-base superalloy was investigated. The results show that after solution treated at 1150 oC, the thicker g ¢ phase is distributed discontinuously in the wider boundary regions in which exists the poor-zone of the finer g ¢ phase. When the solution temperature rises to 1160 oC, the thicker g ¢ phase in the alloy is fully dissolved, and the fine g ¢ phase with high volume fraction is dispersively distributed within the grains, and thereinto the particles of (Nb, Ti)C carbide phase are discontinuously precipitated along the boundaries. After solution treated at 1165 oC, the grain sizes are obviously grown up, and the films of the carbide is continuously precipitated along the boundary. The particle carbides which are discontinuously precipitated along the boundary can effectively pin the grain boundaries and restrain boundaries sliding, resulting in the alloy possessing better enduring properties under the applied stress of 1034 MPa at 650 oC. In the later stage of creep, the deformed characteristic of the alloy is single and double orientation slipping, and the slipping trace on the sample surface increases to bring out the stress concentration as the creep goes on, which results in the initiating and propagating of the micro-cracks along the boundaries up to rupture.

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謝 君,田素貴,周曉明,李晶晶,汪武祥.固溶溫度對FGH95鎳基合金持久斷裂機制的影響[J].稀有金屬材料與工程,2012,41(3):447~451.[Xie Jun, Tian Sugui, Zhou Xiaoming, Li Jingjing, Wang Wuxiang. Effects of Solution Temperatures on Enduring Fracture Mechanism of FGH95 Nickel-Base Superalloy[J]. Rare Metal Materials and Engineering,2012,41(3):447~451.]
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  • 收稿日期:2011-03-30
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