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旋轉(zhuǎn)磁場(chǎng)對(duì)Mg15Al高鋁鎂合金凝固組織的影響
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太原市明星專(zhuān)項(xiàng)基金(09121002);山西省青年科技研究基金(2008021033);山西省歸國(guó)留學(xué)基金(2007-25)


Effect of Rotating Magnetic Field on Solidification Microstructure of Mg15Al High-aluminium Magnesium Alloys
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    摘要:

    利用旋轉(zhuǎn)磁場(chǎng)控制Mg15Al二元高鋁鎂合金凝固過(guò)程,以期獲得均勻細(xì)小的等軸晶,使合金后續(xù)的等通道擠壓能順利進(jìn)行。通過(guò)OM、SEM、EDS測(cè)試手段研究了旋轉(zhuǎn)磁場(chǎng)對(duì)合金凝固組織及溶質(zhì)分配的影響。結(jié)果表明:旋轉(zhuǎn)磁場(chǎng)主要通過(guò)與金屬液流相互作用引起強(qiáng)烈的旋流而產(chǎn)生攪拌作用來(lái)影響合金的溫度場(chǎng)與溶質(zhì)場(chǎng)的分布,故能夠顯著細(xì)化Mg15Al二元高鋁鎂合金組織中的初晶α-Mg,促進(jìn)Al在初晶α-Mg中的固溶,但對(duì)于在凝固末期才形成的共晶組織而言,由于凝固末期所剩液相形不成有效流動(dòng),其形態(tài)受旋轉(zhuǎn)磁場(chǎng)影響不大。隨勵(lì)磁電壓增大,晶粒細(xì)化效果增加,勵(lì)磁電壓為60 V時(shí),晶粒細(xì)化效果最佳,Al在初晶α-Mg中固溶量最高,勵(lì)磁電壓繼續(xù)增加,由于磁場(chǎng)感生熱增加將弱化二次冷卻,使晶粒細(xì)化效果下降。

    Abstract:

    The solidification process of Mg15Al binary magnesium alloy was controlled by the rotating magnetic field (RMF) to obtain even and small equiaxed grains, which make the followed equal channel-angular pressing proceed. The effect of various-strength rotating magnetic field on microstructure and the solute distribution of the Mg15Al binary magnesium alloy was investigated by OM, SEM and EDS. The results show that the distribution of the temperature field and solute field can be obviously improved by the severe fluid flow from the interaction between the RMF and the liquid metal, so the primary phase α-Mg in the as-cast Mg15Al binary alloy can be refined and the solid solution of aluminium in the primary phase α-Mg can be increased by RMF. But the eutectic microstructure has no change by RMF since no effective flow is formed in the end of solidification. The grain refinement increases gradually with the increase of magnetizing voltage. When the magnetizing voltage reaches 60 V, the finest grain and the highest solid solution of aluminium in the primary phase α-Mg can be obtained. But for the magnetizing voltage higher than 60 V, the grain size will decrease partially as the magnetic field-induced heat weakens the secondary cooling.

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王紅霞,梁 偉,謝國(guó)印,龔家林,趙興國(guó),邊麗萍.旋轉(zhuǎn)磁場(chǎng)對(duì)Mg15Al高鋁鎂合金凝固組織的影響[J].稀有金屬材料與工程,2011,40(12):2156~2161.[Wang Hongxia, Liang Wei, Xie Guoyin, Gong Jialin, Zhao Xingguo, Bian Liping. Effect of Rotating Magnetic Field on Solidification Microstructure of Mg15Al High-aluminium Magnesium Alloys[J]. Rare Metal Materials and Engineering,2011,40(12):2156~2161.]
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  • 收稿日期:2010-12-11
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