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退火溫度對Ti-Ni-Cr低溫超彈性合金組織和拉伸性能的影響
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陜西省自然科學(xué)基金 (2009JM6010);陜西省教育廳科研計(jì)劃 (09JK375)


Effects of Annealing Temperatures on Microstructure and Tensile Properties of Ti-Ni-Cr Low-Temperature Superelastic Alloy
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    用光學(xué)顯微鏡和拉伸試驗(yàn)研究了退火溫度 (Ta) 對Ti-50.8Ni-0.3Cr合金顯微組織和拉伸行為的影響。結(jié)果表明,合金原始態(tài)為拉拔纖維組織,退火時(shí)發(fā)生回復(fù)與再結(jié)晶。Ta =350~500 ℃時(shí),為回復(fù)階段,組織呈纖維狀。Ta =550~590 ℃時(shí),為再結(jié)晶階段,纖維組織逐漸變成無畸變等軸晶粒,再結(jié)晶溫度在570 ℃左右。Ta =600~800 ℃時(shí),為晶粒長大階段,顯微組織呈粗大不均勻等軸晶。Ta對合金在低溫 (8 ℃)下的拉伸行為有顯著影響,隨Ta升高,應(yīng)力誘發(fā)馬氏體相變臨界應(yīng)力先降低后升高;350~500 ℃退火態(tài)合金的加工硬化能力和抗拉強(qiáng)度大于550~700 ℃退火態(tài)合金,而后者的延伸率則顯著大于前者。當(dāng)Ta大于650 ℃后合金的延伸率因晶粒粗化而減小

    Abstract:

    effects of annealing temperatures (Ta) on microstructure and tensile behavior of Ti-50.8Ni-0.3Cr (at%) low-temperature superelastic alloy were investigated by optical microscopy and tensile tests. The results show that, the microstructure of the as-received alloy is fibriform, and the recovery and the recrystallization occur in the alloy during annealing. When Ta =350-500 oC, the alloy is at the recovery stage, and the microstructure is fibriform. When Ta =550-590 oC, the alloy is at the recrystallization stage, the microstructure turns to the unstrained equiaxed grains, and the recrystallization temperature of the alloy is about 570 oC. when Ta =600-800 oC, the alloy is at the grain growth stage, the microstructure shows larger and asymmetrical grains. Ta also strongly influences the tensile behavior of the alloy at low temperature (8 oC). With increasing of Ta, the critical stress of the stress-induced martensitic transformation declines at first and then rises; the work hardening ability and the tensile strength of the alloy annealed at 350-500 oC are higher than those of the alloy annealed at 550-700 oC, but the elongation of the latter is significantly larger than that of the former. When Ta >650 oC, the elongation of the alloy decreases due to the grain growth.

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賀志榮,王 啟,王 芳,王永善,楊 軍.退火溫度對Ti-Ni-Cr低溫超彈性合金組織和拉伸性能的影響[J].稀有金屬材料與工程,2011,40(11):1998~2001.[He Zhirong, Wang Qi, Wang Fang, Wang Yongshan, Yang Jun. Effects of Annealing Temperatures on Microstructure and Tensile Properties of Ti-Ni-Cr Low-Temperature Superelastic Alloy[J]. Rare Metal Materials and Engineering,2011,40(11):1998~2001.]
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  • 收稿日期:2010-11-23
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