取向規(guī)則排列;在拉伸蠕變期間,合金中γ′相轉(zhuǎn)變成與[001]取向平行的纖維狀筏形組織。由于施加拉伸載荷,使立方γ¢相中的(100)晶面及γ基體相承受擠壓力,可排斥較大半徑的Al、Ta原子,而在(001)晶面產(chǎn)生較大的晶格擴張應(yīng)變,可誘捕較大半徑的Al、Ta原子,因而促使γ′相沿[001]取向定向生長成為纖維狀筏形組織。在外加應(yīng)力作用下,不同晶面γ′/γ兩相界面的應(yīng)變能密度變化是促使發(fā)生元素擴散和γ′相定向粗化的驅(qū)動力"/>

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一種[011]取向鎳基單晶合金拉伸蠕變中的組織演化
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國家自然科學(xué)基金 (50571070);遼寧省教育廳基金 (2004C004)


Microstructure Evolution of a [011] Orientation Single Crystal Nickel-Base Superalloy during Tensile Creep
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    在1040 ℃,137 MPa下對[011]取向鎳基單晶合金進(jìn)行蠕變曲線測定,采用SEM觀察熱處理及蠕變后樣品不同晶面的組織形貌,研究了[011]取向鎳基單晶合金在蠕變期間的組織演化特征,并分析了組織演化的規(guī)律及影響因素。結(jié)果表明:取向差為4°的[011]取向鎳基單晶合金經(jīng)完全熱處理后,組織是立方γ′相以共格方式嵌鑲在γ基體相中,并沿<100>取向規(guī)則排列;在拉伸蠕變期間,合金中γ′相轉(zhuǎn)變成與[001]取向平行的纖維狀筏形組織。由于施加拉伸載荷,使立方γ¢相中的(100)晶面及γ基體相承受擠壓力,可排斥較大半徑的Al、Ta原子,而在(001)晶面產(chǎn)生較大的晶格擴張應(yīng)變,可誘捕較大半徑的Al、Ta原子,因而促使γ′相沿[001]取向定向生長成為纖維狀筏形組織。在外加應(yīng)力作用下,不同晶面γ′/γ兩相界面的應(yīng)變能密度變化是促使發(fā)生元素擴散和γ′相定向粗化的驅(qū)動力

    Abstract:

    By means of measuring creep curves under the applied stress of 137 MPa at 1040 oC and observing the microstructure by SEM after the alloy was heat treated and crept, the microstructure evolution of [011] orientation single crystal nickel-base superalloy during tensile creep was investigated, and the effect factors of the evolution regularity was analyzed. Results show that, after full heat treatment, the microstructure of [011] oriented single crystal nickel-base superalloy consists of the cubic γ′ phase embedded coherently in the γ matrix, regularly arranged along the <100> orientation. During tensile creep, the cubic γ′ phase in the alloy is transformed into the strip-like rafted structure along the direction parallel to [001] orientation. In the action of the applied tensile stress along the [011] orientation, the extrusion stress is applied on the g phase and (100) crystal plane of the cubic γ′ phase to generate the constricted strain of the lattice, which may exclude the Al and Ta atoms with bigger radius. Whereas, the expanding lattice strain appearing on the (001) crystal plane of the cubic γ′ phase may trap the Al and Ta atoms with bigger radius. Therefore, the cubic γ′ phase is directionally grown into the strip-like rafted structure along the [001] orientation. In the action of the applied stress, the change of the strain energy density in the different interfaces of the cubic γ′/γ phases is thought to be the driving force of the element diffusion and the directional coarsening of γ′ phase

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田素貴,于莉麗,肖 麗,于慧臣,張 姝,錢本江.一種[011]取向鎳基單晶合金拉伸蠕變中的組織演化[J].稀有金屬材料與工程,2011,40(9):1574~1579.[Tian Sugui, Yu Lili, Xiao Li, Yu Huichen, Zhang Shu, Qian Benjiang. Microstructure Evolution of a [011] Orientation Single Crystal Nickel-Base Superalloy during Tensile Creep[J]. Rare Metal Materials and Engineering,2011,40(9):1574~1579.]
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  • 收稿日期:2010-09-28
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