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雙性能渦輪盤用超細(xì)晶坯料制備工藝基礎(chǔ)研究
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    在變形溫度為1130 ℃、模具溫度為1000 ℃的近等溫條件下,通過反復(fù)多方向變形工藝獲得超細(xì)晶粉末高溫合金坯料,平均晶粒直徑約為3 μm,其室溫和750 ℃屈服強(qiáng)度分別高達(dá)1470和1140 MPa。利用OM、SEM和TEM對不同狀態(tài)坯料進(jìn)行微觀組織觀察。結(jié)果表明:在反復(fù)多方向變形的較大累積變形量的作用下,促發(fā)多次完全再結(jié)晶是粉末高溫合金組織充分細(xì)化的直接原因。對比HIP態(tài)原材料,細(xì)晶態(tài)粉末高溫合金的晶界潔凈度更高、厚度更薄,微空洞等體積缺陷更少,并且有細(xì)小的第三級γ′相彌散分布于基體之中。

    Abstract:

    Ultrafine-grained PM superalloy billet with approximate grain size of 3 μm was prepared by multiple forging under the near isothermal condition of 1130 oC deformation temperature and 1000 oC mould temperature, and the yield strengths at room temperature and 750 oC reach 1470 MPa and 1140 MPa, respectively. Otherwise, the microstructure evolution was observed by OM, SEM and TEM. The results indicate that the full refinement of the PM superalloy is directly caused by the entire recrystallization of many times resulting from great accumulative deformation of multiple forging. Compared with HIPed original material, the ultrafine-grained PM superalloy possesses fine tertiary γ' phases dispersed in the matrix, cleaner and thinner boundary, which present less defects such as micropores.

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寧永權(quán),姚澤坤,郭鴻鎮(zhèn),陶 宇,張義文.雙性能渦輪盤用超細(xì)晶坯料制備工藝基礎(chǔ)研究[J].稀有金屬材料與工程,2010,39(7):1235~1239.[Ning Yongquan, Yao Zekun, Guo Hongzhen, Tao Yu, Zhang Yiwen.[J]. Rare Metal Materials and Engineering,2010,39(7):1235~1239.]
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  • 收稿日期:2009-08-15
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