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La2O3對鐓粗Mo棒的橫向組織和塑性的影響
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國家高新技術發(fā)展“863”計劃項目(2006AA03Z517);湖南省自然科學基金(05JJ30095


Effects of La2O3 on Transverse Microstructure and Ductility of Upset Mo Bars
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    摘要:

    利用鍛造鐓粗工藝制備了高橫向塑性的純Mo和Mo-La2O3棒,檢測了其在不同溫度退火后的橫向彎曲性能并觀察了其組織結(jié)構(gòu)。結(jié)果表明:純Mo棒經(jīng)鍛造鐓粗變形85%后橫向具有較好的塑性,延伸率達到了5%;而同狀態(tài)下的Mo-La2O3棒只有2%。這是因為此狀態(tài)下純Mo棒中的位錯可動性要好。隨著退火溫度的升高,純Mo棒和Mo-La2O3棒的橫向塑性都逐漸升高,Mo-La2O3棒的最大橫向延伸率大于純Mo棒(超過10%)。Mo-La2O3棒橫向塑性的提高與La2O3粒子鈍化微裂紋有關。在退火過程中,鐓粗純Mo棒和Mo-La2O3棒都發(fā)生了回復再結(jié)晶過程,位錯組態(tài)變化一致,鐓粗過程中產(chǎn)生了大量位錯胞,隨著退火溫度的升高而逐步消失

    Abstract:

    Pure Mo and Mo-La2O3 bars with high transverse ductility were prepared by forging and upsetting. The microstructure and transverse bending properties of both bars were investigated after different annealing treatments. The results show that the pure Mo bars forged and upset by 85% possess good transverse ductility and the elongation reaches 5%, while that of the forged and upset Mo-La2O3 bars is only 2%. It is because the mobility of dislocations in the Mo bars is better than that of Mo-La2O3 bars in this condition. As the annealing temperature increases, the transverse ductility of the two kinds of bars is improved gradually; particularly the elongation of Mo-La2O3 bars annealed at 1200 oC for 1 h exceeds 10%, higher than that of pure Mo bars. In the upsetting process, many dislocation cells can be observed in the Mo-La2O3 bars, which disappeared little by little as the annealing temperature increased, and still there were a lot of tangled dislocations in the cells which were pinned by the dispersed La2O3 particles. The improvement of the transverse ductility of Mo-La2O3 bars is relative with the interaction between the La2O3 particles and dislocations. Both the Mo bars and Mo-La2O3 bars have recovery recrystallization process, and similar dislocation structure change

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陳 暢,汪明樸,譚 望,張 娟,金 鵬,張 真. La2O3對鐓粗Mo棒的橫向組織和塑性的影響[J].稀有金屬材料與工程,2010,39(4):638~641.[Chen Chang, Wang Mingpu,,Tan Wang, Zhang Juan, Jin Peng, Zhang Zhen. Effects of La2O3 on Transverse Microstructure and Ductility of Upset Mo Bars[J]. Rare Metal Materials and Engineering,2010,39(4):638~641.]
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  • 收稿日期:2009-04-29
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