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鈦合金片層α相在熱加工過(guò)程中演變規(guī)律的定量研究
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Quantitative Analysis on Microstructural Evolution of Lamellar α Phase in Titanium Alloy during Hot Working
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Key Foundational Research Plan of China (2007CB613807); Program for New Century Excellent Talents in University (NCET-07-0696); the Fund of the State Key Laboratory of Solidification Processing in NWPU (35-TP-2009)

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    摘要:

    對(duì)具有片層α相的Ti-17合金圓餅在兩相區(qū)進(jìn)行5種變形程度的等溫鍛造及固溶時(shí)效處理,用定量金相學(xué)方法研究了片層α相在熱加工過(guò)程中的演變規(guī)律。研究發(fā)現(xiàn):α相的厚度隨著應(yīng)變量的增大而增大;變形程度及圓餅的變形區(qū)域?qū)Ζ料嘈螒B(tài)的變化有很大影響。隨變形程度的增大,α相的形態(tài)參數(shù)Feret Ratio (Feretmax/Feretmin)的分布曲線在Feret Ratio介于1.5~2.5區(qū)間出現(xiàn)單峰,且峰值不斷增大,大Feret Ratio的α相比例逐漸減小。圓餅中心位置的Feret Ratio分布曲線具有較大的峰值。大變形使片層α相的等軸化程度提高,改善了圓餅的組織均勻性。等效應(yīng)變對(duì)組織中不同形態(tài)α相分布的影響曲線表明:球化α相比例隨著等效應(yīng)變的增大呈單調(diào)增大,增大速率表現(xiàn)為慢—快—極慢的分階段特征;近等軸狀的α相比例先快速增長(zhǎng)后不斷減少;片層狀和大片層狀α相比例隨著等效應(yīng)變?cè)龃蟪蕟握{(diào)減少。片層α相的臨界球化與完全球化的等效應(yīng)變分別約為0.4與1.0

    Abstract:

    To quantitatively research the microstructural evolution of lamellar α phase in titanium alloys, large size cakes of Ti-17 alloy with initial lamellar microstructure were isothermally-forged at different strains in α+β phase field followed by solid-solution and aging treatment. The changes of α thickness and morphology in different locations (center, midradius, edge) of the cakes deformed to different strain levels were measured and the imposed strain was estimated using finite element analysis. It is found that increasing of forging strains causes an increase in thickness of α phase. The modification of α morphology depends strongly on the forging strains and the locations in the cakes. The distribution curves of α morphology parameter Feret Ratio were characterized by no peak at lower strains, and a single peak appears at Feret Ratio 1.5-2.5 at larger strains. Moreover, the peak values increased with increasing of the height reduction, and the distribution curves at the center have the largest peak values. Increasing of forging strains will cause the high-Feret-Ratio lamellae to decrease but low-Feret-Ratio α to increase noticeably. Sufficiently imposed strains also can improve the microstructure homogeneity in different locations of the cakes. The effect of the effective strains on the percentage of α phase with different morphologies is also quantificationally summarized. The average strains for initiation of globalization are of the order of 0.4 and those for completion are of the order of 1.0, which are lower than that of conventional α+β titanium alloys

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王凱旋,曾衛(wèi)東,趙永慶,邵一濤,周建華,王曉英,周義剛.鈦合金片層α相在熱加工過(guò)程中演變規(guī)律的定量研究[J].稀有金屬材料與工程,2010,39(4):565~569.[Wang Kaixuan, Zeng Weidong, ZhaoYongqing, Shao Yitao, Zhou Jianhua, Wang Xiaoying, Zhou Yigang. Quantitative Analysis on Microstructural Evolution of Lamellar α Phase in Titanium Alloy during Hot Working[J]. Rare Metal Materials and Engineering,2010,39(4):565~569.]
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  • 收稿日期:2009-04-28
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