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短切SiCf/LAS復合材料的顯微結(jié)構(gòu)與介電性能
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Microstructure and Dielectric Properties of Chopping SiCf/LAS Composites
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The National Natural Science Foundation of China (50572090)

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    摘要:

    采用熱壓燒結(jié)法制備出致密的短切SiCf增強LAS玻璃陶瓷復合材料,并討論保溫時間與熱壓壓力對復合材料介電性能的影響。結(jié)果表明,測試頻率在8~12 GHz之間,復合材料復介電常數(shù)實部ε′由基體的7.6上升到10~100,虛部ε″由基體的0.34上升到40~160,介電損耗tgδ由基體的0.04上升到1~20,并具有明顯的頻散效應。隨保溫時間的延長或熱壓壓力的提高,復合材料ε′增大,ε″與tgδ減小。此外,斷口形貌的SEM觀察表明,隨保溫時間的延長或熱壓壓力的提高,復合材料界面層變厚。

    Abstract:

    The chopping SiCf/LAS composites were prepared by the hot-pressing method. The effects of hot-pressing time and pressures on the microstructures and the dielectric properties of the composites were researched. Compared with the LAS matrix and the SiC fibre, the results of dielectric constant testing in the range of 8-12 GHz indicate that the dielectric constant real part, imaginary part and dielectric dissipation of all samples increase by 1-3 orders of magnitude, and show obvious frequency dispersion effect. Their real parts increase while their imaginary parts and dielectric dissipations decline with the increase of the hot-pressing time or pressures. The SEM fractographs show that the composite interfacial films between the fibre and the matrix are thickened with the increase of the hot-pressing time or pressures.

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翟曉勇,周萬城,羅 發(fā),朱冬梅.短切SiCf/LAS復合材料的顯微結(jié)構(gòu)與介電性能[J].稀有金屬材料與工程,2009,38(12):2089~2092.[Zhai Xiaoyong, Zhou Wancheng, Luo Fa, Zhu Dongmei. Microstructure and Dielectric Properties of Chopping SiCf/LAS Composites[J]. Rare Metal Materials and Engineering,2009,38(12):2089~2092.]
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  • 收稿日期:2008-11-21
  • 最后修改日期:2008-12-24
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