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粉末冶金Ta合金中的隱性胞狀結(jié)構(gòu)
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TG146.4

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Hidden Cell Structure in Powder Metallurgy Ta Alloys
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    摘要:

    采用Ta-W-Hf預(yù)合金化粉末通過冷等靜壓成型、熱等靜壓和高溫退火工藝制備了Ta—W-Hf合金塊材,討論了熱等靜壓和后續(xù)的高溫退火處理對(duì)合金性能的影響。發(fā)現(xiàn)在低的熱等靜壓溫度下,材料具有較高的強(qiáng)度和硬度,但塑性較低;提高熱等靜壓溫度或進(jìn)行高溫退火處理,可以大幅度提高拉伸延伸率和斷面收縮率,同時(shí)伴隨著強(qiáng)度的降低。分析表明,產(chǎn)生這種現(xiàn)象的主要原因是合金中的氧元素在原料顆粒中分布不均勻,并保留在熱等靜壓成形后的塊體材料中,形成了一個(gè)無相變的隱性硬殼的胞狀結(jié)構(gòu)。高溫退火處理可以消除這種結(jié)構(gòu)。

    Abstract:

    Using pre-alloying Ta-W-Hf powder,Ta-W-Hf bulk alloys were prepared by means of CIP(cold isostatic press),HIP(hot isostatic press)and high temperature annealing.This paper is focused on the influences of HIP and high temperature annealing on the alloy performances.The results show that high strength,high hardness and low plasticity appear for the alloy after HIP at low temperature.The elongation and section shrinking would be largely improved and the strength would be decreased after HIP at high temperature or high temperature annealing due to the oxygen element's inhomogeneous distribution in the raw material particles and remaining in the bulk after HIP to form the hidden harden cell structures without phase change in these regions.These cell structures would disappear after high temperature annealing.

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張小明 張廷杰 胡忠武 李晴宇 譚栓斌 殷為宏.粉末冶金Ta合金中的隱性胞狀結(jié)構(gòu)[J].稀有金屬材料與工程,2006,35(8):1243~1246.[Zhang Xiaoming, Zhang Tingjie, Hu Zhongwu, Li Qingyu, Tan Shuanbin, Yin Weihong. Hidden Cell Structure in Powder Metallurgy Ta Alloys[J]. Rare Metal Materials and Engineering,2006,35(8):1243~1246.]
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  • 收稿日期:2005-05-31
  • 最后修改日期:2006-04-28
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