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原位反應(yīng)自發(fā)滲透法TiC/AZ91D鎂基復(fù)合材料及AZ91D鎂合金的拉伸變形與斷裂行為
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TB331 TG113.251

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中國科學(xué)院金屬研究所新入所骨干人員科研啟動基金,遼寧省自然科學(xué)基金(20032012)及教育部留學(xué)回國人員科研啟動基金資助


Tensile Deformation and Fracture Behavior of AZ91D Magnesium Alloy and TiC/Mg Magnesium Matrix Composites Synthesized by in situ Reactive Infiltration Technique
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    摘要:

    利用原位反應(yīng)自發(fā)滲透技術(shù)合成了47.5%碳化鈦TiC(體積分?jǐn)?shù),下同)增強(qiáng)AZ91D鎂基復(fù)合材料,對比研究了該復(fù)合材料與鑄態(tài)鎂合金AZ91D基體的室溫與高溫拉伸變形行為,觀察了拉伸斷口微觀組織形貌,并分析了這兩種材料的斷裂特征。結(jié)果表明,TiC/Mg復(fù)合材料具有良好的高溫力學(xué)性能,在拉伸變形速率為0.001s^-1以及溫度為723K,時其拉伸強(qiáng)度可達(dá)91.1MPa,而此時相同變形條件下的鑄態(tài)AZ91D鎂合金拉伸斷裂強(qiáng)度只有41.1MPa,增幅達(dá)120%。而在室溫下,鎂基復(fù)合材料的拉伸斷裂強(qiáng)度僅高出基體鑄態(tài)鎂合金23.4%。鎂基復(fù)合材料的斷裂應(yīng)變較低,高低溫時均表現(xiàn)為脆性斷裂;而鎂合金則由室溫下的脆性斷裂向高溫下的韌性斷裂過渡。

    Abstract:

    A newly developed cost-effective processing route, in situ reactive infiltration technique, was utilized to fabricate 47.5vol.%TiC/AZ91D magnesium matrix composites. A comparative study was made on the tensile deformation behavior at room and elevated temperatures for the as synthesized composites and the matrix alloy magnesium AZ91D and their fracture characteristics were also analyzed as well. The results show that the TiC/Mg composites fabricated by in situ reactive infiltration process possess excellent high-temperature mechanical properties. The ultimate tensile strength of the matrix magnesium alloy AZ91D at 723 K and a strain rate of 0.001 s^-1 is 41.1 MPa, while that of TiC/Mg composites at the same deformation conditions increases by 120% and reaches 91.1 MPa. At room temperature, the ultimate tensile strength of the composites increases only by 23.4% as compared with the AZ91D alloy. The SEM observation of the morphologies for the fractured surfaces reveals that the fracture mode differs from one another in that the composites are of brittle characteristic at room and elevated temperatures due to its limited failure strain, whereas the fracture mode of the magnesium alloy has a transition from brittleness at room temperature towards ductileness at elevated temperature.

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陳禮清 郭金花 王繼杰 徐永波 畢敬.原位反應(yīng)自發(fā)滲透法TiC/AZ91D鎂基復(fù)合材料及AZ91D鎂合金的拉伸變形與斷裂行為[J].稀有金屬材料與工程,2006,35(1):29~33.[Chen Liqing, Guo Jinhua, Wang Jijie, Xu Yongbo, Bi Jing. Tensile Deformation and Fracture Behavior of AZ91D Magnesium Alloy and TiC/Mg Magnesium Matrix Composites Synthesized by in situ Reactive Infiltration Technique[J]. Rare Metal Materials and Engineering,2006,35(1):29~33.]
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  • 收稿日期:2004-09-20
  • 最后修改日期:2005-01-31
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