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Al-10Mg二元合金系燒結過程的原位觀察
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TF124.5

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科技部重大基礎研究前期研究專項(02061005),國家自然科學基金(59771016)資助項目


In-Situ Investigation of the Sintering Process of Al and Mg Binary Alloy System
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    摘要:

    燒結是粉末冶金工藝中至關重要的一環(huán),為了加強對燒結過程的直觀認識,利用高溫光學顯微鏡(HTOM)對Al-10Mg的二元純金屬粉末體系進行了燒結的原位觀察試驗,發(fā)現該體系燒結的典型物理過程是:鎂顆粒邊界熔化,鎂晶界熔化,最后為鎂顆粒熔化;鎂顆粒熔化進程不同步;當燒結溫度超過某一臨界溫度Tc時,鎂顆粒迅速熔化;而且燒結速度隨冷坯密度的提高而加快,這為進一步合理優(yōu)化燒結工藝提供了直接的參照依據.

    Abstract:

    Sintering is one of the most important steps for powder metallurgy (PM). In order to observe the sintering process directly, a high temperature optical microscope (HTOM) was used to in-situ investigate the Al and Mg binary alloy system with a weight ratio of 9:1. A typical physical evolving character was found in this system. The melting process of magnesium particles is not synchronous, first from the particle border, then in the grain boundary, and last into the whole magnesium particle. When sintering temperature is above a critical temperature Tc, the magnesium particle melts in a very short time, and the sintering rate is accelerated with the increasing of the cold compact density. These experiment results afford a direct reference to the sintering routine optimization.

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張文興 柴東朗 郗雨林 周敬恩. Al-10Mg二元合金系燒結過程的原位觀察[J].稀有金屬材料與工程,2005,34(3):489~492.[. In-Situ Investigation of the Sintering Process of Al and Mg Binary Alloy System[J]. Rare Metal Materials and Engineering,2005,34(3):489~492.]
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  • 最后修改日期:2004-04-26
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