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工藝參數(shù)對(duì)陽(yáng)極弧放電等離子體制備鎳納米粉的影響
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TB383

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甘肅省科技攻關(guān)基金資助(502-041211)


Effects of Technology Parameters of Anodic Arc Discharged Plasma on Preparation of Ni Nanopowders
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    摘要:

    在Ar惰性保護(hù)氣氛中,采用陽(yáng)極弧放電等離子方法用自行研制的裝置制備出了高純Ni納米粉末。研究了在制備過(guò)程中電弧電流、氣體壓力等工藝參數(shù)對(duì)納米粉產(chǎn)率及粒度的影響。利用XRD、TEM對(duì)制得的樣品的形貌、晶體結(jié)構(gòu)、粒度及其分布進(jìn)行測(cè)定。結(jié)果表明,適當(dāng)控制某些工藝參數(shù)就能制取粒徑范圍在20nm~100nm的納米粉,在其它工藝參數(shù)不變條件下,氣壓升高或電弧電流增大,都會(huì)使粒度增大,產(chǎn)率提高。

    Abstract:

    In inert gas, pure Ni nanopowders were prepared by anodic arc discharged plasma method utilizing self-designed and fabricated experimental apparatus, and the influence of arc current and gas pressure on the production rate and particle size of metal nanopowders in the process was studied. The product was characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and the corresponding electron diffraction (ED) to determine the morphology, crystal microstructure, the size and size distribution. The experiment results revealed that Ni nanopowders with particle size range from 20 nm to 100 nm can be obtained by using the suitable controlled experimental apparatus. The production rate and particle size increase with raising arc current or gas pressure when other factors are fixed. The crystal structure of Ni nanopowders is the same as the bulk materials, is fcc phase.

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魏智強(qiáng) 溫賢倫 王君 吳志國(guó) 徐建偉 吳現(xiàn)成 閆鵬勛.工藝參數(shù)對(duì)陽(yáng)極弧放電等離子體制備鎳納米粉的影響[J].稀有金屬材料與工程,2004,33(3):305~308.[Wei Zhiqiang, Wen Xianlun, Wang Jun, Wu Zhiguo, Xu Jianwei, Wu Xiancheng, Yan Pengxun. Effects of Technology Parameters of Anodic Arc Discharged Plasma on Preparation of Ni Nanopowders[J]. Rare Metal Materials and Engineering,2004,33(3):305~308.]
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  • 最后修改日期:2002-08-26
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