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不同制備工藝對金屬鈦粉微觀性質(zhì)及應用的影響研究
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1:浙江工業(yè)職業(yè)技術學院2:浙江工業(yè)大學特種裝備制造與先進加工技術教育部/浙江重點實驗室

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浙江省教育廳高等學校訪問工程師校企合作項目(FG2018143);; 紹興市科技計劃項目(2018C10003)


Study on Effect of Different Preparation Processes on the Micro Properties and Application of Titanium Powder
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    摘要:

    金屬鈦粉末在增材制造等新型成形方法中得到越來越廣泛的應用,目前主要通過熔鹽電解法和氣體霧化法來制取。借助X射線衍射技術(XRD)、掃描電鏡(SEM)、比表面積測試(BET)、熱重-差熱分析法(TGA-DSC)等檢測方法,從物相結(jié)構(gòu)、晶胞參數(shù)、微觀形貌、表面狀態(tài)、熱穩(wěn)定性等方面,對采用熔鹽電解和氣體霧化2種不同工藝制取的金屬鈦粉的性質(zhì)和應用進行全面對比分析。結(jié)果表明,電解鈦粉微觀形貌不規(guī)則,同一性差,適合作為粉末冶金原料和熱還原劑;氣霧化鈦粉微觀形貌為均勻球狀,表面不易吸附氣體雜質(zhì),比表面積為3.69 m~2/g,更適宜作為增材制造的原材料。

    Abstract:

    Titanium powder is more and more widely used in new forming methods such as additive manufacturing, and it is mainly produced by molten salt electrolysis and gas atomization at present. The properties and applications of titanium powder prepared by the two different preparation processes were comprehensively compared and analyzed by means of X-ray diffraction(XRD), scanning electron microscope(SEM), Brunauer Emmett Teller(BET), thermogravimetry analysis and differential scanning calorimeter(TGA-DSC) from the phase structure, cell parameters, micro morphology, surface state, thermal stability and other aspects. The results show that the morphology of the titanium powder produced by molten salt electrolysis is irregular and the identity is poor, which is suitable for powder metallurgy raw material and thermal reducing agent. And the microstructure of atomized titanium powder is uniform and spherical, and the specific surface area is 3.69 m~2/g, which is more suitable for additive manufacturing.

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李紅莉;張宇;.不同制備工藝對金屬鈦粉微觀性質(zhì)及應用的影響研究[J].鈦工業(yè)進展,2020,37(6):29-33.

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  • 在線發(fā)布日期: 2021-01-12
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