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退火溫度對鉿棒組織與性能的影響
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國防基礎(chǔ)科研計劃資助項目(XNJK19-07)


Effects of Annealing Temperature on Microstructure and Properties of Hafnium Bars
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    摘要:

    采用熱軋加冷旋鍛的方式將φ60 mm鉿棒坯加工至φ13.3 mm,然后分別在440、600、740、900、1 040℃下保溫1 h進行真空退火處理,對比研究了不同退火溫度下鉿棒的顯微組織、室溫及高溫拉伸性能、高溫拉伸斷口形貌。結(jié)果表明,隨著退火溫度的升高,晶粒逐漸長大,但孿晶組織并不會隨著退火溫度升高而完全消失,相反,在高溫退火時鉿棒組織中容易形成退火孿晶;鉿棒的抗拉強度、屈服強度隨著退火溫度的升高逐漸降低,抗拉強度的降速出現(xiàn)了先慢后快的現(xiàn)象,屈服強度反之。440、600、740℃高溫拉伸斷口形貌為多韌窩態(tài)的韌性斷裂,韌窩大小、密度略有不同,而900、1 040℃退火后,斷口形貌存在解理臺階并有河流狀花紋,為脆性斷裂。

    Abstract:

    The φ60 mm hafnium billet was processed to φ13.3 mm by hot rolling and cold rotary forging,and then vacuum annealing was carried out at 440,600,740,900 and 1 040℃for 1 h respectively.The microstructure,room temperature and high temperature tensile properties,high temperature tensile fracture morphology of the hafnium bars under different annealing temperatures were studied comparatively.It is shown that with the increase of annealing temperature,the grain gradually grows,but the twin structure does not completely disappear with the increase of annealing temperature,in contrast,annealed twins are easily developed in the hafnium bar at high temperature;the tensile strength and yield strength of the hafnium bar gradually decrease with the increase of the annealing temperature,with a slow and then fast decline of the tensile strength while the yield strength is otherwise.The tensile fracture morphologies at 440,600 and 740℃present ductile fracture feature with many dimples,whose fracture size and density are slightly different.However,after annealing at 900℃and 1 040℃,the fracture morphologies appear as cleavage steps and river-like pattern,which are brittle fractures.

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蔡文博;武宇;姚修楠;趙鴻磊;陳昊;楊娟;朱波;.退火溫度對鉿棒組織與性能的影響[J].鈦工業(yè)進展,2020,37(5):31-35.

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  • 在線發(fā)布日期: 2020-11-09
  • 出版日期: 2020-10-25