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鈦及鈦合金的新型多級深度熱還原技術(shù)
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A Novel Multi-stage Deep Thermal Reduction Technology for Titanium and Its Alloys
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    摘要:

    提出了"多級深度熱還原"的理念,即鎂/鋁熱自蔓延-多級深度還原制備鈦及鈦合金技術(shù),利用該技術(shù)成功制備出純度為99.69%的高純還原鈦粉,氧含量<0.15%的Ti6Al4V合金粉;制備出20 kg級的Ti Al合金鑄錠,其Ti/Al原子比為1∶1,氧含量為0. 09%。該研究成果已在山東淄博傅山企業(yè)集團(tuán)推廣應(yīng)用,所建成的200 t/a鈦粉生產(chǎn)線于2019年12月全線貫通投產(chǎn)。實踐證明,該技術(shù)有效解決了傳統(tǒng)金屬熱還原無法徹底還原TiO_2直接制備鈦及鈦合金的難題,可使鈦材生產(chǎn)成本降低30%左右,為鈦材低成本清潔制備與應(yīng)用奠定了工業(yè)化基礎(chǔ)。

    Abstract:

    The concept of 'multi-stage deep thermal reduction' was proposed,the technology of magnesium/aluminum thermal self-propagating high-temperature synthesis( SHS) multi-stage deep reduction to prepare titanium and its alloys.The high purity reduced titanium powder with purity of 99. 69%,Ti-6Al-4V powder with oxygen content less than 0. 15% and TiAl alloy ingot of 20 kg scale( the atomic ratio of Ti/Al was 1∶1) with oxygen content 0. 09% were successfully prepared with this technology. The achievements have been successfully transformed and applied in Shandong Fushan Group. The 200 t/a reduced titanium powder industrial demonstration line was successfully put into operation on December,2019. This technology solves the problem that traditional metallothermic reduction can not completely reduce TiO_2 to directly prepare titanium and its alloys,which can reduce the production cost of titanium by about 30%,and lay an industrial foundation for low-cost clean preparation and application of titanium materials.

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張廷安;豆志河.鈦及鈦合金的新型多級深度熱還原技術(shù)[J].鈦工業(yè)進(jìn)展,2020,37(2):43-48.

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  • 在線發(fā)布日期: 2020-06-04
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